Buchwald, Stephen L.
LaMaire, Susan J.
Nielsen, Ralph B.
Watson, Brett T.
King, Susan M.

A Modified Procedure for the Preparation of Cp2Zr(H)Cl (Schwartz’s Reagent)

“,
Tet. Lett.
,
1987
,
28
(
34
)
,
3895-3898
.
Abstract

A convenient method for the preparation of 65–85 g quantities of Cp2Zr(H)Cl, Schwartz's reagent has been developed. The reagent prepared by this method is of high purity and has several advantages over the reagent prepared by previously reported methods.